Enzymatic desymmetrization of meso-1α,4α-dihydroxy-cis-decalins
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Add time:09/09/2019 Source:sciencedirect.com
The stereoselective acetylation of meso-decalindiols 1 and 2 by vinyl acetate in the presence of Candida antarctica lipase gave monoester (1R,4S,4aR,8aS)-5 and (1R,4S,4aR,8aS)-6 in high enantiomeric excess (ee ⩾98%). The hydrolysis of the corresponding meso-diacetates 3 and 4 in the presence of porcine liver esterase in phosphate buffer provided the opposite enantiomers.
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