Low temperature synthesis of CHLORINE PENTAFLUORIDE (cas 13637-63-3) using dioxygen difluoride
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Add time:09/06/2019 Source:sciencedirect.com
CHLORINE PENTAFLUORIDE (cas 13637-63-3) has been prepared successfully in high purity by the fluorination of ClF3 at −78°C with dioxygen difluoride. The yield of ClF5 by this method is quantitative. The procedure illustrates the general utility of O2F2 in high valent fluoride synthesis.
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