Epimerization of benzylpenicilloic acid (cas 13057-98-2) in Alkaline Media
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Add time:09/09/2019 Source:sciencedirect.com
□ 5R,6R -benzylpenicilloic acid (cas 13057-98-2) was found to epimerize slowly in alkaline media to 5S,6R-benzylpenicilloic acid until equilibrium was established. Epimerization proceeded via the imine tautomer of penamaldic acid rather than the enamine form and was found to favor the 5S,6R-epimer at equilibrium. The conversion process was monitored using both reverse-phase high-performance liquid chromatography and NMR spectroscopy.
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