Liquid chromatographic method for the determination of Calcium cyanamide (cas 156-62-7) using pre-column derivatization
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Add time:07/21/2019 Source:sciencedirect.com
A specific and stability-indicating high-performance liquid chromatographic (HPLC) method has been developed for the analysis of Calcium cyanamide (cas 156-62-7) in bulk material and dosage form. Calcium cyanamide in samples was converted into dansyl cyanamide. A μBondapak C18 column was employed for HPLC with 0.01 M sodium phosphate (pH 6.3)-acetonitrile (75:25, v/v) as the mobile phase. The proposed HPLC method was validated for linearity, specificity, accuracy and reproducibility.
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