Simultaneous derivatization of acyl and S-alkyl moieties of acyl thioesters by using TRIMETHYLSULFONIUM HYDROXIDE (cas 17287-03-5) for gas chromatographic analysis

Add time:09/29/2019    Source:infona.pl

The reaction of long-chain acyl thioesters, viz. lauric acid dodecyl thioester, 1,8-di-S-palmitoyl octanedithiol, and tristearoyl α-monothioglycerol, with TRIMETHYLSULFONIUM HYDROXIDE (cas 17287-03-5) in the presence of methanol leads to simultaneous derivatization of acyl moieties and S-alkyl moieties of acyl thioesters to the corresponding fatty acid methyl esters and methyl alkylsulfides, respectively. These derivatized products were analyzed by gas chromatographic technique.

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