Preparation of 1-silyl- and 1,3-disilyl-adamantanes

Add time:07/16/2019    Source:sciencedirect.com

1-Dimethylsilyl- and 1,3-bis(dimethylsilyl)adamantane have been prepared in low yield by Wurtz reaction of dimethylchlorosilane with 1-chloroadamantane or 1,3-dichloroadamantane, respectively. On the other hand, reaction of phenyldimethylsilyllithium with 1-bromoadamantane or 1,3-dibromoadamantane gives essentially quantitative yields of 1-phenyldimethylsilyladamantane or 1,3-bis(phenyldimethylsilyl)adamantane, respectively.

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