Catalytic—enthalpimetric determination of diethyldithiocarbamate (DDTC) and nickel(II) using the iodine—azide reaction
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Add time:07/20/2019 Source:sciencedirect.com
An enthalpimetric method for the determination of diethyldithiocarbamate (DDTC) based on the catalysis of the iodine—azide reaction is proposed. The behaviour of those metal ions which inhibit the catalytic activity of DDTC by complex formation is also studied, and a simple and rapid procedure for the determination of trace amounts of nickel(II) is described. The relative standard deviations are within 2 and 3% for concentration levels of 2×10−5 M DDTC and 2×10−6 M nickel(II), respectively.
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