Welcome to LookChem.com Sign In|Join Free
  • or
Home > Products >  > 

3-Amino-6-methylbenzenesulfonamide
Related Products

Hot Products

Basic Information Post buying leads Suppliers Cas Database
Name

3-Amino-6-methylbenzenesulfonamide

 EINECS 691-180-5
CAS No. 6973-09-7 Density 1.359 g/cm3
PSA 94.56000 LogP 2.58690
Solubility N/A Melting Point 163-164℃
Formula C7H10N2O2S Boiling Point 421.5 °C at 760 mmHg
Molecular Weight 186.235 Flash Point 208.7 °C
Transport Information N/A Appearance N/A
Safety Risk Codes N/A
Molecular Structure Molecular Structure of 6973-09-7 (3-Amino-6-methylbenzenesulfonamide) Hazard Symbols N/A
Synonyms

3-Aminosulfonyl-4-methylaniline;5-Amino-2-methylbenzenesulfonamide;NSC 36969;

Article Data 17

3-Amino-6-methylbenzenesulfonamide Synthetic route

200266-64-4

4-acetylamino-toluene-2-sulfonic acid amide

6973-09-7

5-amino-2-methylbenzenesulfonamide

Conditions
ConditionsYield
With hydrogenchloride for 0.333333h; Heating;75%
With hydrogenchloride
4-nitro-toluene-sulfonic acid-(2)-amide

4-nitro-toluene-sulfonic acid-(2)-amide

6973-09-7

5-amino-2-methylbenzenesulfonamide

Conditions
ConditionsYield
With ammonium sulfide
103-89-9

4-Methylacetanilide

6973-09-7

5-amino-2-methylbenzenesulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 67 percent / conc. aq. NH4OH
2: 75 percent / 18percent aq. HCl / 0.33 h / Heating
View Scheme
6269-91-6

4-nitrotoluene-2-sulfonamide

6973-09-7

5-amino-2-methylbenzenesulfonamide

Conditions
ConditionsYield
With hydrogenchloride; tin(ll) chloride In diethylene glycol dimethyl ether; water for 0.75h;
With hydrogen; palladium 10% on activated carbon In methanol; dichloromethane under 2585.81 Torr; for 0.25h;
palladium-carbon In methanol; dichloromethane
99-99-0

1-methyl-4-nitrobenzene

6973-09-7

5-amino-2-methylbenzenesulfonamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: chlorosulfonic acid / 24 h / 0 - 110 °C
2: ammonium hydroxide / water; ethyl acetate / 20 °C
3: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 0.25 h / 2585.81 Torr
View Scheme
Multi-step reaction with 2 steps
1.1: chlorosulfonic acid / 24 h / 0 - 110 °C
1.2: 20 °C
2.1: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 0.25 h / 2585.81 Torr
View Scheme
Multi-step reaction with 3 steps
1: chlorosulfonic acid / 24 h / 0 - 110 °C
2: ammonium hydroxide / ethyl acetate / 20 °C
3: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 0.25 h / 2585.81 Torr
View Scheme
Multi-step reaction with 2 steps
1: chlorosulfonic acid / 24 h / 0 - 110 °C
2: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 0.25 h / 2585.81 Torr
View Scheme
121-02-8

2-methyl-5-nitrobenzene-1-sulfonyl chloride

6973-09-7

5-amino-2-methylbenzenesulfonamide

Conditions
ConditionsYield
With palladium on activated charcoal In tetrahydrofuran at 100℃; for 8h; Temperature; Solvent; Reagent/catalyst;
Multi-step reaction with 2 steps
1: ammonium hydroxide / ethyl acetate / 20 °C
2: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 0.25 h / 2585.81 Torr
View Scheme
6973-09-7

5-amino-2-methylbenzenesulfonamide

555-16-8

4-nitrobenzaldehdye

5-(p-Nitrobenzylideneamino)-2-toluenesulfonamide

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 0.0166667h; Irradiation;98%
444731-75-3

2,3-dimethyl-N-(2-chloropyrimidin-4-yl)-N-methyl-2H-indazole-6-amine

6973-09-7

5-amino-2-methylbenzenesulfonamide

pazopanib hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In isopropyl alcohol Reflux;97%
Stage #1: N-(2-chloropyrimidin-4-yl)-N-methyl-2,3-dimethyl-2H-indazole-6-amine; 5-amino-2-methylbenzenesulfonamide In ethanol at 68 - 72℃; for 3h;
Stage #2: With hydrogenchloride In 1,4-dioxane; ethanol at 68 - 72℃; for 0.0333333h; Product distribution / selectivity;		96.4%
Stage #1: N-(2-chloropyrimidin-4-yl)-N-methyl-2,3-dimethyl-2H-indazole-6-amine; 5-amino-2-methylbenzenesulfonamide In ethanol at 68 - 72℃; for 3h; Heating / reflux;
Stage #2: With hydrogenchloride In 1,4-dioxane; ethanol at 68 - 72℃; for 8h;		96.4%
698-63-5

5-nitrofurane-2-carboxaldehyde

6973-09-7

5-amino-2-methylbenzenesulfonamide

5-(5'-Nitro-2'-furfurylideneamino)-2-toluenesulfonamide

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 0.0333333h; Irradiation;96%
7147-77-5

5-(4-nitrophenyl)-2-furaldehyde

6973-09-7

5-amino-2-methylbenzenesulfonamide

5-[5'-(p-Nitrophenyl)-2'-furfurylideneamino]-2-toluenesulfonamide

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 0.0333333h; Irradiation;96%

3-Amino-6-methylbenzenesulfonamide Chemical Properties

IUPAC Name: 5-Amino-2-methylbenzenesulfonamide
Synonyms of Benzenesulfonamide,5-amino-2-methyl- (CAS NO.6973-09-7): 2-Methyl-5-aminobenzene sulfonamide ; 3-Amino-6-methylbenzenesulfonamide ; 5-Amino-2-methylbenzene sulfonamide ; Benzenesulfonamide, 5-amino-2-methyl- (9CI) ; 3-Amino-6-Methylbenzenesulfona ; 3-Amino-6-methylbenzenesulfonamide,99+% ; 3-amino-6-methyl benzene sulphonamide
CAS NO: 6973-09-7
Molecular Formula of Benzenesulfonamide,5-amino-2-methyl- (CAS NO.6973-09-7): C7H10N2O2S
Molecular Weight: 186.2315
Molecular Structure:

Polar Surface Area: 49 Å2
Index of Refraction: 1.609
Molar Refractivity: 47.43 cm3
Molar Volume: 136.9 cm3
Surface Tension: 58.8 dyne/cm
Density of Benzenesulfonamide,5-amino-2-methyl- (CAS NO.6973-09-7): 1.359 g/cm3
Flash Point: 208.7 °C
Enthalpy of Vaporization: 67.55 kJ/mol
Boiling Point: 421.5 °C at 760 mmHg
Vapour Pressure: 2.6E-07 mmHg at 25°C 

Post a RFQ

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

1

What can I do for you?
Get Best Price

Get Best Price for 6973-09-7