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Cas Database |
| Name |
1,3-Bis(3-aminophenoxy)benzene |
EINECS | 234-082-6 |
| CAS No. | 10526-07-5 | Density | 1.243 g/cm3 |
| PSA | 70.50000 | LogP | 5.59800 |
| Solubility | Insoluble in water | Melting Point |
108 °C |
| Formula | C18H16N2O2 | Boiling Point | 479.9 °C at 760 mmHg |
| Molecular Weight | 292.337 | Flash Point | 264.8 °C |
| Transport Information | N/A | Appearance | N/A |
| Safety | 26-36/37/39 | Risk Codes | 20/21/22 |
| Molecular Structure |
|
Hazard Symbols | 20/21/22:; |
| Synonyms |
Aniline,3,3'-(m-phenylenedioxy)di- (7CI,8CI);1,3-Bis(3-aminophenoxy)benzene;1,3-Bis(m-aminophenoxy)benzene;3,3'-(m-Phenylenedioxy)dianiline;3,3'-Phenylenedioxydianiline;3,3'-[1,3-Phenylenebis(oxy)]bis[aniline];3,3'-[m-Phenylenebis(oxy)]dianiline;APB;APB-N; |
Article Data | 7 |
1,3-Bis(3-aminophenoxy)benzene Synthetic route
- 54060-31-0
1,3-bis(3-nitrophenoxy)benzene
- 10526-07-5
1,3-bis (3-aminophenoxy)-benzene
| Conditions | Yield |
|---|---|
| With 5%-palladium/activated carbon; hydrogen In ethanol under 15001.5 Torr; for 8h; | 94% |
| Conditions | Yield |
|---|---|
| With potassium hydroxide; copper at 200 - 280℃; |
- 10526-07-5
1,3-bis (3-aminophenoxy)-benzene
| Conditions | Yield |
|---|---|
| With water-d2; platinum on carbon; palladium 10% on activated carbon at 180℃; for 24h; | 98% |
- 10526-07-5
1,3-bis (3-aminophenoxy)-benzene
- 106-89-8
epichlorohydrin
| Conditions | Yield |
|---|---|
| Stage #1: 1,3-bis (3-aminophenoxy)-benzene; epichlorohydrin With lanthanum nitrate hexahydrate In 1,2-dichloro-ethane; isopropyl alcohol at 70 - 87℃; for 3h; Stage #2: With sodium hydroxide In 1,2-dichloro-ethane; isopropyl alcohol at 70 - 75℃; for 0.75h; | 96% |
- 10526-07-5
1,3-bis (3-aminophenoxy)-benzene
- 1107-00-2
4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride
| Conditions | Yield |
|---|---|
| In 1-methyl-pyrrolidin-2-one at 20℃; for 36h; | 90% |
| Conditions | Yield |
|---|---|
| at 100℃; for 1.33333h; Sealed tube; | 90% |
- 10526-07-5
1,3-bis (3-aminophenoxy)-benzene
- 38775-52-9
diethyl 2,2'-(sulfonylbis(4,1-phenylene)bis(oxy))diacetate
| Conditions | Yield |
|---|---|
| In ethanol at 80℃; Solvent; | 90% |
- 10526-07-5
1,3-bis (3-aminophenoxy)-benzene
- 1107-00-2
4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride
- polymer, polyimide, Mw (GPC): ca. 10800, Mw/Mn (GPC): ca. 2.2; monomer(s): 1,3-bis(3-aminophenoxy)benzene; 3,5-diaminobenzyl alcohol dihydrochloride; 4,4'-(hexafluoroisopropylidene)diphthalic anhydride
polymer, polyimide, Mw (GPC): ca. 10800, Mw/Mn (GPC): ca. 2.2; monomer(s): 1,3-bis(3-aminophenoxy)benzene; 3,5-diaminobenzyl alcohol dihydrochloride; 4,4'-(hexafluoroisopropylidene)diphthalic anhydride
| Conditions | Yield |
|---|---|
| Stage #1: 1,3-bis (3-aminophenoxy)-benzene; 3,5-diaminobenzyl alcohol dihydrochloride; 4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride In 1-methyl-pyrrolidin-2-one at 0℃; for 6h; Stage #2: With aniline In 1-methyl-pyrrolidin-2-one at 20℃; for 30h; Stage #3: In 1-methyl-pyrrolidin-2-one; toluene at 150℃; Further stages.; | 87% |
| Conditions | Yield |
|---|---|
| Stage #1: methoxymethanol; 1,3-bis (3-aminophenoxy)-benzene In methanol at 20℃; Inert atmosphere; Stage #2: para-tert-butylphenol In methanol at 90℃; for 6h; Inert atmosphere; | 81% |
- 5470-96-2
quinoline 2-carbaldehyde
- 10526-07-5
1,3-bis (3-aminophenoxy)-benzene
| Conditions | Yield |
|---|---|
| In methanol for 11h; | 53% |
1,3-Bis(3-aminophenoxy)benzene Specification
The IUPAC name of Benzenamine,3,3'-[1,3-phenylenebis(oxy)]bis- is 3-[3-(3-aminophenoxy)phenoxy]aniline . With the CAS registry number 10526-07-5, it is also named as 3,3'-(m-Phenylenebis(oxy))dianiline ; 1,3-Bis(3-aminophenoxy)benzene ; 1,3-Phenylenebis(3-oxyaniline) ; 3,3'-[1,3-Phenylenebis(oxy)]dianiline . The product's categories are aromatic hydrocarbons (substituted) & derivatives, miscellaneous, diphenyl ethers (for high-performance polymer research), functional materials and reagent for high-performance polymer research.
The Benzenamine,3,3'-[1,3-phenylenebis(oxy)]bis- is harmful by inhalation, in contact with skin and if swallowed. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. If you want to contact this product, you must wear suitable protective clothing, gloves and eye/face protection.
The other characteristics of this product can be summarized as: (1)ACD/LogP: 3.05 ; (2)# of Rule of 5 Violations: 0 ; (3)ACD/LogD (pH 5.5): 3.02 ; (4)ACD/LogD (pH 7.4): 3.05 ; (5)ACD/BCF (pH 5.5): 115.02 ; (6)ACD/BCF (pH 7.4): 122.02 ; (7)ACD/KOC (pH 5.5): 1021.71 ; (8)ACD/KOC (pH 7.4): 1083.9 ; (9)#H bond acceptors: 4 ; (10)#H bond donors: 4 ; (11)#Freely Rotating Bonds: 6 ; (12)Index of Refraction: 1.667 ; (13)Molar Refractivity: 87.61 cm3 ; (14)Molar Volume: 235.1 cm3 ; (15)Polarizability: 34.73×10-24 cm3 ; (16)Surface Tension: 55.2 dyne/cm ; (17)Enthalpy of Vaporization: 74.43 kJ/mol ; (18)Vapour Pressure: 2.27E-09 mmHg at 25°C ; (19)Rotatable Bond Count: 4 ; (20)Exact Mass: 292.121178 ; (21)MonoIsotopic Mass: 292.121178 ; (22)Topological Polar Surface Area: 70.5 ; (23)Heavy Atom Count: 22.
People can use the following data to convert to the molecule structure. SMILES: O(c1cc(N)ccc1)c3cccc(Oc2cccc(N)c2)c3; InChI: InChI=1/C18H16N2O2/c19-13-4-1-6-15(10-13)21-17-8-3-9-18(12-17)22-16-7-2-5-14(20)11-16/h1-12H,19-20H2; InChIKey: DKKYOQYISDAQER-UHFFFAOYAA. Benzenamine,3,3'-[1,3-phenylenebis(oxy)]bis- has many suppliers, such as Changzhou Sunlight Pharmaceutical Co., Ltd.. The price of this product changes with the market.
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