Related Products
- 3,10-Diaminotricyclo(5.2.1.0(sup 2,6))decane
- 3,10-Dinitrophenanthrene
- 3-((10-ETHYL-11-(p-HYDROXYPHENYL)DIBENZ-(B,F)OXEPIN-3-YL)OXY)-1,2-PROPANEDIOL HYDRATE (4:1)
- 3-(1,1,2,2-Tetrafluoroethoxy)aniline
- 3-(1,1,2,2-Tetrafluoroethoxy)benzaldehyde
- 3-(1,1,2,2-Tetrafluoroethoxy)bromobenzene
- 3-(1,1,2,2-Tetrafluoroethoxy)toluene
- 3-[1,1'-Biphenyl]-4-yl-1,2,3,4-tetrahydro-1-naphthol
- 3,11-Dichloro-6,11-dihydro-6-methyldibenzo[c,f][1,2]thiazepine 5,5-dioxide
- 3-[(1,1-Dimethyl-2-hydroxyethyl)amino]-2-hydroxypropanesulfonicacid
- 626-41-5Phenol,3,5-dibromo-
- 62642-59-54-Diethylaminomethylbenzoic acid
- 62642-62-0Benzoicacid, 4-(4-morpholinylmethyl)-
- 626-43-7Benzenamine, 3,5-dichloro-
- 6264-40-01,3,4-Thiadiazole-2(3H)-thione,5-(methylthio)-
- 626-44-8Benzene, 1,3,5-triiodo-
- 6264-66-01,2-Benzenediamine,4-(4-aminophenoxy)-
- 6264-67-11,3-Benzenediamine,4-fluoro-
- 6264-69-34-Bromobenzene-1,3-diamine
- 626-48-22,4-Dihydroxy-6-methylpyrimidine
Hot Products
- 104987-11-3Tacrolimus
- 141-53-7Sodium formate
- 8001-54-5Quaternary ammonium compounds, alkylbenzyldimethyl, chlorides
- 9003-39-8Povidone
- 10161-34-9Trenbolone acetate
- 402957-28-2Telaprevir
- 68-19-9Cyanocobalamin
- 7631-86-9Silicon dioxide
- 302-79-4Tretinoin
- 77-92-9Citric acid
|
Basic Information |
|
Post buying leads |
|
Suppliers |
|
Cas Database |
| Name |
3,5-Dibromoaniline |
EINECS | N/A |
| CAS No. | 626-40-4 | Density | 2.022g/cm3 |
| PSA | 26.02000 | LogP | 3.37500 |
| Solubility | N/A | Melting Point |
56.5oC |
| Formula | C6H5 Br2 N | Boiling Point | 296.8oC at 760 mmHg |
| Molecular Weight | 250.92 | Flash Point | 133.3oC |
| Transport Information | N/A | Appearance | N/A |
| Safety | Risk Codes | N/A | |
| Molecular Structure |
|
Hazard Symbols |
 Xi
|
| Synonyms |
Aniline,3,5-dibromo- (6CI,7CI,8CI); 3,5-Dibromoaniline; 3,5-Dibromobenzenamine; NSC6216 |
Article Data | 29 |
3,5-Dibromoaniline Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; tin at 90℃; for 7h; | 99% |
| With hydrogenchloride; hydrogen; nickel In ethanol | 96% |
| Stage #1: 3,5-dibromonitrobenzene With tin(II) chloride dihdyrate In tetrahydrofuran; methanol at 60℃; for 20h; Stage #2: With water; sodium hydroxide for 2h; | 90% |
Conditions
| Conditions | Yield |
|---|---|
| With bis(triphenylphosphine)nickel(II) chloride; lithium hexamethyldisilazane In toluene at 100℃; for 2h; Glovebox; Sealed tube; | 81% |
- 626-40-4
3,5-dibromoaniline
Conditions
| Conditions | Yield |
|---|---|
| With O-(2,4-dinitrophenyl)hydroxylamine In toluene at 100℃; for 30h; Inert atmosphere; | 56% |
- 7647-01-0
hydrogenchloride
- 5326-51-2
N,N'-bis-(3,5-dibromo-phenyl)-hydrazine
A
- 626-40-4
3,5-dibromoaniline
B
- 38292-74-9
3,3′,5,5′-tetrabromo-1,1′-azobenzene
Conditions
| Conditions | Yield |
|---|---|
| at 150℃; im Rohr; |
- 5326-51-2
N,N'-bis-(3,5-dibromo-phenyl)-hydrazine
- 7664-93-9
sulfuric acid
A
- 626-40-4
3,5-dibromoaniline
B
- 860599-94-6
2,6,2',6'-tetrabromo-benzidine
C
- 854242-36-7
4,6,2',6'-tetrabromo-biphenyl-2,4'-diyldiamine
D
- 38292-74-9
3,3′,5,5′-tetrabromo-1,1′-azobenzene
...Expand
Conditions
| Conditions | Yield |
|---|---|
| bei der Reduktion; |
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1.1: NaNO2; H2SO4; aq. H3PO4 / 2 h 1.2: urea; H2SO4; aq. H3PO4 / 20 °C 1.3: 85 percent / H2SO4; aq. H3PO4 / 0 - 20 °C 2.1: 99 percent / tin; aq. HCl / 7 h / 90 °C View Scheme | |
| Multi-step reaction with 2 steps 1: 80 percent / H2SO4; NaNO2 / ethanol / 36 h / 90 °C 2: 89 percent / SnCl2*2H2O / ethanol; tetrahydrofuran / 20 h / 20 °C View Scheme | |
| Multi-step reaction with 2 steps 1: 97 percent / NaNO2, H2SO4 / ethanol 2: 96 percent / 1.) H2; 2.) aq. HCl / Raney Ni / ethanol View Scheme |
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: 97 percent / Br2 / acetic acid / 4 h / 65 °C 2: 80 percent / H2SO4; NaNO2 / ethanol / 36 h / 90 °C 3: 89 percent / SnCl2*2H2O / ethanol; tetrahydrofuran / 20 h / 20 °C View Scheme | |
| Multi-step reaction with 3 steps 1: diluted hydrochloric acid; bromine 3: tin; hydrochloric acid View Scheme | |
| Multi-step reaction with 3 steps 1: aqueous sulfuric acid; bromine 3: iron; diluted sulfuric acid View Scheme | |
| Multi-step reaction with 3 steps 1.1: acetic acid; bromine / 4 h / 65 °C 2.1: sulfuric acid; sodium nitrite / ethanol / 40 h / 80 °C 3.1: tin(II) chloride dihdyrate / methanol; tetrahydrofuran / 20 h / 60 °C 3.2: 2 h View Scheme |
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: 98 percent / Br2 / acetic acid 2: 97 percent / NaNO2, H2SO4 / ethanol 3: 96 percent / 1.) H2; 2.) aq. HCl / Raney Ni / ethanol View Scheme |
3,5-Dibromoaniline Chemical Properties
IUPAC Name:3,5-dibromoaniline
Molecular Formula:C6H5Br2N
Molecular Weight:250.918600 g/mol
Density:2.022 g/cm3
Flash Point:133.3 °C
Enthalpy of Vaporization:53.66 kJ/mol
Boiling Point:296.8 °C at 760 mmHg
Vapour Pressure:0.0014 mmHg at 25 °C
storage temp.:keep Cold
Synonyms of 3,5-Dibromoaniline(626-40-4):
benzenamine, 3,5-dibromo-;3,5-Dibromoaniline
Categories of 3,5-Dibromoaniline(626-40-4):Amines;blocks;Bromides
3,5-Dibromoaniline Safety Profile
Safety Information of 3,5-Dibromoaniline(626-40-4):
Hazard Codes:Xi
Hazard Codes:Xi
Post a RFQ
1
What can I do for you?
Get Best Price
Get Best Price for 626-40-4
3,5-Dibromoaniline
