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Cas Database |
| Name |
4-Methoxybenzyl bromide |
EINECS | 608-101-7 |
| CAS No. | 2746-25-0 | Density | 1.406 g/cm3 |
| PSA | 9.23000 | LogP | 2.59010 |
| Solubility | N/A | Melting Point |
240 °C |
| Formula | C8H9BrO | Boiling Point | 241.6 °C at 760 mmHg |
| Molecular Weight | 201.063 | Flash Point | 95.6 °C |
| Transport Information | UN 3265 8/PG 2 | Appearance | N/A |
| Safety | 26-36/37/39-45 | Risk Codes | 34 |
| Molecular Structure |
|
Hazard Symbols |
 C
|
| Synonyms |
(4-Methoxyphenyl)methyl bromide;1,4-Methoxybromomethylbenzene;(4-Bromomethylphenoxy)methane;Anisole,p-(bromomethyl)- (6CI,7CI,8CI);1-(Bromomethyl)-4-methoxybenzene;4-(Bromomethyl)anisole;4-Methoxy-1-(bromomethyl)benzene;p-(Bromomethyl)anisole;p-Methoxybenzyl bromide; |
Article Data | 168 |
4-Methoxybenzyl bromide Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen bromide In benzene at 78℃; for 1h; Bromination; | 100% |
| With hydrogen bromide In benzene at 78℃; for 1h; | 100% |
| With phosphorus tribromide In diethyl ether at 0℃; for 2h; | 100% |
Conditions
| Conditions | Yield |
|---|---|
| With dihydrogen peroxide; methyltrioxorhenium(VII); sodium bromide In acetic acid for 10h; Ambient temperature; | A 99% B 1% |
Conditions
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide; dibenzoyl peroxide In Diethyl carbonate for 0.25h; Reflux; Microwave irradiation; | 98% |
| With sodium bromate; 2,2'-azobis-(2,4-dimethylvaleronitrile); sulfuric acid; sodium bromide In dichloromethane; water Reflux; | 92% |
| With N-Bromosuccinimide; trityl tetrafluoroborate In dichloromethane; benzene at 20℃; Irradiation; Inert atmosphere; chemoselective reaction; | 75% |
Conditions
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide; dibenzoyl peroxide In various solvent(s) at 90 - 95℃; for 1h; Wohl-Ziegler bromination; | A 95% B 5% |
- 18494-82-1
2-(4-methoxy-benzyloxy)-tetrahydro-pyran
- 2746-25-0
p-Methoxybenzyl bromide
Conditions
| Conditions | Yield |
|---|---|
| With 4-aminophenyl diphenylphosphinite; bromine In dichloromethane at 20℃; for 0.5h; | 95% |
- 14629-56-2
trimethyl(4-methoxybenzyloxy)silane
- 2746-25-0
p-Methoxybenzyl bromide
Conditions
| Conditions | Yield |
|---|---|
| With 4-aminophenyl diphenylphosphinite; bromine In dichloromethane at 20℃; | 95% |
Conditions
| Conditions | Yield |
|---|---|
| With bromine; trimethylamine borane In chloroform at 0 - 5℃; for 0.0333333h; | 86% |
| With chloro-trimethyl-silane; 1,1,3,3-Tetramethyldisiloxane; lithium bromide; zinc(II) chloride In acetonitrile at 80℃; for 0.25h; | 84% |
| With Dichloromethylsilane; phosphorus tribromide; iron(III) chloride In acetonitrile for 4h; Heating; | 55% |
- 631-61-8
ammonium acetate
- 105-13-5
4-Methoxybenzyl alcohol
A
- 104-21-2
p-methoxybenzyl acetate
B
- 2746-25-0
p-Methoxybenzyl bromide
Conditions
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide; triphenylphosphine In acetonitrile at 20℃; for 1.9h; Cooling with ice; | A 86% B 6% |
- 92565-78-1
4-methoxy-1-(methoxymethoxy)methyl benzene
- 2746-25-0
p-Methoxybenzyl bromide
Conditions
| Conditions | Yield |
|---|---|
| With tetrabutylammomium bromide; 1-(n-butyl)-3-methylimidazolium tetrachloroindate at 135 - 140℃; for 0.0916667h; Microwave irradiation; Neat (no solvent); chemoselective reaction; | 81% |
- 101803-60-5
tert-butyl((4-methoxybenzyl)oxy)dimethylsilane
- 1034-39-5
dibromotriphenylphosphorane
- 2746-25-0
p-Methoxybenzyl bromide
Conditions
| Conditions | Yield |
|---|---|
| In dichloromethane for 15h; Ambient temperature; | 80% |
4-Methoxybenzyl bromide Chemical Properties
Product Name: 4-Methoxybenzyl bromide
Synonyms: METHOXYBENZYLBROMIDE(4-);1-(BROMOMETHYL)-4-METHOXYBENZENE;4-METHOXYBENZYL BROMIDE;4-MethoxybenzylBromide4-Methoxybenzylbromide;p-Methoxybenzylbromide;4-Methoxybenzyl bromide ,95%
MF: C8H9BrO
MW: 201.06
bp : 91 °C1 mm Hg(lit.)
density : 1.379 g/mL at 25 °C(lit.)
refractive index : n20/D 1.5780(lit.)
Fp : >230 °F
Synonyms: METHOXYBENZYLBROMIDE(4-);1-(BROMOMETHYL)-4-METHOXYBENZENE;4-METHOXYBENZYL BROMIDE;4-MethoxybenzylBromide4-Methoxybenzylbromide;p-Methoxybenzylbromide;4-Methoxybenzyl bromide ,95%
MF: C8H9BrO
MW: 201.06
bp : 91 °C1 mm Hg(lit.)
density : 1.379 g/mL at 25 °C(lit.)
refractive index : n20/D 1.5780(lit.)
Fp : >230 °F
4-Methoxybenzyl bromide Safety Profile
Risk Statements : 34
Safety Statements : 26-36/37/39-45
Hazard Codes : C
RIDADR : UN 3265 8/PG 2
WGK Germany : 1
Transport Information : UN 3265
Safety Statements : 26-36/37/39-45
Hazard Codes : C
RIDADR : UN 3265 8/PG 2
WGK Germany : 1
Transport Information : UN 3265
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4-Methoxybenzyl bromide
