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463-52-5

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Iodine Catalyzed Oxidative Coupling of Diaminoazines and Amines for the Synthesis of 3,5-Disubstituted-1,2,4-Triazoles
A simple, convenient, transition metal-free one pot synthesis of 3,5-disubstituted-1,2,4-triazoles has been established. The innovation in this reaction is the use of easily available 1,1-diaminoazines as substrates. This method provides the products with wider substrate scope, at an expedited rate, and with relatively better yields in comparison to the reported methods. The reaction mechanism involves an initial intermolecular nucleophilic addition (facilitated by I2) followed by intramolecular nucleophilic cyclization.
Beifuss, Uwe,Bharatam, Prasad V.,Chourasiya, Sumit S.,Kathuria, Deepika,Sahoo, Subash C.,Wani, Aabid A.
p. 7659 - 7671
(2021/06/25)

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Chemical Properties

Melting Point: 81°C
Boiling Point: 46.3 °C at 760 mmHg
Flash Point:°C
Density: 1.07 g/cm³
PKA: 11.60±0.40(Predicted)
PSA: 49.87000
LogP: 0.35220

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