Journal of Organic Chemistry p. 1078 - 1082 (1987)
Update date:2022-07-29
Topics:
Kosugi, Hiroshi
Kitaoka, Masaki
Tagami, Katsuya
Takahashi, Akira
Uda, Hisashi
1-Alkynylmagnesium bromides react cleanly and stereospecifically with (-)-menthyl (-)-(S)-p-toluenesulfinate (2) in toluene to produce chiral 1-alkynyl p-tolyl (+)-(S)-sulfoxides 5a-d in high yields.Reduction of 5a-d with lithium aluminum hydride in THF a
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