Bulletin of the Chemical Society of Japan p. 3466 - 3467 (1991)
Update date:2022-07-30
Topics:
Okamoto, Hidenori
Kato, Shozo
The reduction of N-<(3-methoxy-2-thienyl)methylene>-2,6-dimethylaniline (2) by use of trichlorosilane proceeded smoothly in the presence of a catalytic amount of BF3*Et2O.The trichlorosilane/BF3*Et2O combination was applicable to the reduction of various Schiff bases.In the case of dichlorosilane, the reduction of 2 proceeded with a 90percent yield without any catalysts.
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