Tetrahedron Letters p. 2033 - 2036 (1987)
Update date:2022-07-29
Topics: Optical purity Protecting groups Purification Final steps Stereochemistry Control Starting Materials Halogenation Hydroxylation
Okamoto, Sentaro
Shimazaki, Toshiyuki
Kobayashi, Yuichi
Sato, Fumie
Kinetic resolution of γ-trimethylsilyl allylic alcohols 5 by the Sharpless process combined with the reactivity of epoxysilyl or vinylsilyl compounds affords a highly efficient method for preparation of optically pure γ-halo secondary allylic alcohols of type 1-4 and propargylic alcohols 14, thus providing a practical route to the prostaglandin ω-chain.
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