Tetrahedron Letters p. 2033 - 2036 (1987)
Update date:2022-07-29
Topics: Optical purity Protecting groups Purification Final steps Stereochemistry Control Starting Materials Halogenation Hydroxylation
Okamoto, Sentaro
Shimazaki, Toshiyuki
Kobayashi, Yuichi
Sato, Fumie
Kinetic resolution of γ-trimethylsilyl allylic alcohols 5 by the Sharpless process combined with the reactivity of epoxysilyl or vinylsilyl compounds affords a highly efficient method for preparation of optically pure γ-halo secondary allylic alcohols of type 1-4 and propargylic alcohols 14, thus providing a practical route to the prostaglandin ω-chain.
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Doi:10.1016/S0040-4039(00)85169-2
(1986)Doi:10.1021/acs.joc.7b01746
(2017)Doi:10.1021/ol8020435
(2008)Doi:10.1002/hlca.19510340131
(1951)Doi:10.1016/S0040-4039(00)95734-4
(1987)Doi:10.1021/ol802745n
(2009)
