Tetrahedron p. 5097 - 5104 (1986)
Update date:2022-08-04
Topics:
Brown, John M.
Cook, Stephen J.
Kent, Alexander G.
The ligands 2,3,4-tri-O-methyl-6-(diphenylphosphino)-α-D-glucopyranosyl-2',3',4'-tri-O-methyl-6'-(diphenylphosphino)-α-D-glucopyranoside (αα-TREDIP) and the anomer ββ-TREDIP have been prepared from dimesylate precursors.They form a range of rhodium complexes in wich the phosphines can be mutually cis or trans, depending on the other ligands present.The αα-anomer shows more propensity for trans-complexation then the ββ-anomer, and this may be explained on conformational grounds.
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