A ONE-STEP PREPARATION OF (E)-4-MERCAPTO-2-BUTENOIC ESTERS AND NITRILES RELATIVE MICHAEL REACTIVITIES IN SIMPLE UNSATURATED SYSTEMS

DOI: 10.1016/S0040-4039(00)85271-5

Source and publish data:

Tetrahedron Letters p. 5583 - 5586 (1986)

Update date:2022-08-04

Topics:

Authors:

Bunce, Richard A.

Pierce, Joey D.

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1016/S0040-4039(00)85271-5

A one-step procedure is described for the preparation of (E)-4-mercapto-2-butenoic esters and nitriles in 75-85percent yield.The corresponding ketones could not be isolated due to dimerization of the initially-formed products by a double Michael reaction.

Full text of DOI:10.1016/S0040-4039(00)85271-5

Products guided by the article

Product name:2-[5-(2-Oxo-2-phenyl-ethyl)-[1,4]dithian-2-yl]-1-phenyl-ethanone

Cas No:109202-05-3

R&D Labs maybe for 109202-05-3

Jurong Huaheng Natural Biological Products Factory

website:http://www.risebiochem.com

Contact:+86-13921007726

Address:Chuncheng town,Jurong city,Jiangsu province,China
Valiant Fine Chemicals Co., Ltd.

Contact:+86 535 6101878/6374484

Address:11 Wuzhishan Rd.,YTETDZ,Yantai,264006,Shandong,China
Yancheng Creator Chemical Co., Ltd

Contact:0086-515-88710008 88710068 88710858 88710868

Address:No.21 Renming Road, Longgang Town, Yandu County,Yancheng City
NIGNXIA XINDACHANG TECHNOLOGY CO.,LTD

Contact:86-0951-7815345

Address:North side of Qiyuan Road, west side of Yuanfeng Highway, New Material Park, Ningdong Energy and Chemical Industry Base, Ningxia,China
Hubei Xiangxi Chemical Industry Co.,Ltd

Contact:+86-710-3454830

Address:No.7, Daqing East Road, Xiangfan City, Hubei Province, China

Relevant to this article

Synthesis and evaluation of C2-carbon-linked heterocyclic-5-hydroxy-6-oxo-dihydropyrimidine-4-carboxamides as HIV-1 integrase inhibitors

Doi:10.1016/j.bmcl.2014.11.060
(2015)
Doi:10.1021/jo01363a029
(1957)
Stereoselective synthesis of 2-aminocyclobutanols via photocyclization of α-amido alkylaryl ketones: Mechanistic implications for the Norrish/Yang reaction

Doi:10.1021/ja0111941
(2002)
Preparation of (4,4-difluoro-1,2,3,4-tetrahydro-5H-1-benzazepin-5-ylidene)acetamide derivatives as novel arginine vasopressin V₂ receptor agonists

Doi:10.1016/j.bmc.2008.09.039
(2008)
Synthesis and self-assembly of oligo(p-phenylenevinylene) peptide conjugates in water

Doi:10.1002/chem.201002495
(2011)
Synthesis, spectroscopic study and crystal structure determination by x-ray powder diffractometry of CdCl₂(TzTn)J [TzTn=2-(3,4-dichlorophenyl) imino-N(2-thiazolin-2-yl)tetrahydro-l,3-thiazine]

Doi:10.1002/zaac.200700159
(2007)

Article Doi