Journal of Organic Chemistry p. 9458 - 9460 (2008)
Update date:2022-08-03
Topics:
Gold, Henrik
Van Delft, Pieter
Meeuwenoord, Nico
Codee, Jeroen D. C.
Filippov, Dmitri V.
Eggink, Gerrit
Overkleeft, Herman S.
Van Der Marel, Gijs A.
(Chemical Equation Presented) A new method for the construction of pyrophosphates is reported based on the coupling of a sugar phosphate and a nucleoside phosphoramidite. The in situ formed phosphate-phosphite intermediate was subsequently oxidized with tBuOOH. Three UDP-N-acetylglucosamine derivatives were prepared using this one-pot procedure in good yields.
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