Tetrahedron Letters p. 1677 - 1680 (1987)
Update date:2022-07-30
Topics: Allylation
Shimizu, Makoto
Nakahara, Yuko
Kanemoto,Shigekazu
Yoshioka, Hirosuke
Fluoromethyl ketone enol ethers are regiospecifically prepared in good yields by treatment of 2-alkoxy-1,3-bis(t-butyldimethylsiloxy)alkene with TBAF-MsF, and subsequent thermal (3,3)-sigmatropic rearrangement on the 2-alkenyl enol ethers gives α-allylate
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