Synthesis p. 149 - 153 (1987)
Update date:2022-08-04
Topics:
Tercio, J.
Ferreira, B.
Catani, V.
Comasseto, J. V.
A new general synthesis of 2,2-dimethyl-2H-thiochromenes in good yield consists of the Michael addition of thiophenols to 3-methyl-2-butenoic acid, intramolecular cyclocondensation of the resultant 3-methyl-3-phenylthiobutanoic acids, reduction of the 2,2-dimethyl-4-oxothiochromenes thus obtained with sodium borohydride, and acid-catalyzed dehydration of the resultant 4-hydroxy-2,2-dimethylthiochromans.
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Doi:10.1021/jo01063a002
(1961)Doi:10.1007/BF00762001
(1987)Doi:10.1271/bbb.80100
(2008)Doi:10.1016/S0040-4039(00)95377-2
(1987)Doi:10.1016/S0040-4020(01)89973-7
(1987)Doi:10.1246/cl.1987.113
(1987)