Synthesis p. 503 - 505 (1987)
Update date:2022-08-04
Topics:
Fetizon, Marcel
Goulaouic, Pierre
Hanna, Issam
The tertiary allylic alcohols obtained from lithiated dihydro-1,4-dioxin and ketones, 2-(1-hydroxyalkyl)-5,6-dihydro-1,4-dioxins, react with 1,2-ethanedithiol and 1,3-propanedithiol in dichloromethane in the presence of catalytic amounts of ether-boron trifluoride to give, after acid hydrolysis, 2-acyl-1,3-dithiolanes or 2-acyl-1,3-dithianes, respectively, i.e., 2-oxoalkanal 1-dithioacetals.
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Doi:10.1016/S0040-4039(00)94321-1
(1990)Doi:10.1021/acs.orglett.6b03158
(2016)Doi:10.1016/S0040-4039(00)95492-3
(1987)Doi:10.1080/00397919508015845
(1995)Doi:10.1016/S0040-4039(01)80974-6
(1987)Doi:10.1016/S0040-4020(01)81439-3
(1988)
