Efficient one-pot synthesis of 2-chloro-1,1, 1-trifluoro-2-alkenes under solvent-free conditions

DOI: 10.1080/00397910802431123

Source and publish data:

Synthetic Communications p. 756 - 763 (2009)

Update date:2022-09-26

Topics:

Authors:

Chen, Mu-Wang

Zhang, Xing-Guo

Zhong, Ping

Hu, Mao-Lin

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Article abstract of DOI:10.1080/00397910802431123

The improved one-pot Wittig reaction had been used to prepare trifluoromethyl-containing olefins under solvent-free conditions. Treatment of aldehydes with PPh3 and CF3CCl3 in the presence of K2CO3 at 100°C afforded 2-chloro-1,1,1-trifluoro-2-alkenes in g

Full text of DOI:10.1080/00397910802431123

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