Tetrahedron p. 2675 - 2680 (1987)
Update date:2022-08-03
Topics:
Eritja, Ramon
Ziehler-Martin, J.Paige
Walker, Peter A.
Lee, Terry D.
Legesse, Kassu
Albericio, Fernando
Kaplan, Bruce E.
The utilization of the Nα-fluorenylmethoxycarbonyl derivative of S-t-butyl sulphenyl cysteine in solid-phase peptide synthesis for the preparation of several cysteine-containing peptides is described. When this derivative is located in the C-terminal position a side reaction prevents the formation of the desired product. Finally, a peptide containing a disulphide bond has been obtained in excellent yields by selective deprotection of the cysteines and disulfide bond formation on the solid support.
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