Chemistry of Heterocyclic Compounds p. 1324 - 1329 (1987)
Update date:2022-07-30
Topics:
Kriven'ko, A. P.
Nikolaeva, T. G.
Yudovich, L. M.
Komyagin, N. T.
Yanovskii, A. I.
et al.
The configurations of the perhydroacridines formed in the catalytic hydroamination of threo-methylenedicyclohexanone and the product of its cyclization - 2-hydroxy-2,3-tetramethylenebicyclo<3.3.1>nonan-9-one - were established by means of the 13C NMR spectra and alternative synthesis.It is shown that isomers with cis-anti-cis and cis-syn-cis configurations are formed as a result of the reactions.The results of X-ray diffraction analysis are presented for cis-syn-cis-N-(2-hydroxyethyl)perhydroacridine.
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