Synthesis p. 303 - 306 (1988)
Update date:2022-09-26
Topics:
Dieter, R. Karl
Lugade, Ananda G.
Methyl p- and o-hydroxydithiobenzoates were prepared regiospecifically in a one-pot procedure from phenol methyl- and methoxymethyl,ethers, respectively.The p-hydroxy compounds were prepared by treatment of the methyl ethers with carbon disulfide, methyl iodide, and aluminum chloride.The second procedure involves ortho-metallation, carbon disulfide dithiocarboxylation, sulfur alkylation with methyl iodide, and in situ phenol deprotection with aluminum chloride/methyl iodide.
View MoreJinan Hongfangde Pharmatech Co.,Ltd
Contact:86-531-88870908
Address:F Bldg. West Unit North Area of Univ. Tech. Garden Xinyu Rd. Jinan New & High Tech Industry Development Zone Shandong, China
Nanjing Habo Medical Technology Co., Ltd.
Contact:025-85769882
Address:No.108. Ganjiabian east. Qixia District .Nanjing
Anhui Xinyuan Technology Co.,Ltd
website:http://www.ahxytech.com/
Contact:0086-559-3515800
Address:Huangshan City of Anhui Province Huizhou Huizhou District Road, 21-9
Zhangjiagang Jianing Import & Export Co.,Ltd.
Contact:086-512-55379012 13913607595
Address:NO.1 Guotai North Road Zhangjiagang Economic Development Zone,215600,Jiangsu,China
Contact:+86-10-67147360/67107388
Address:No.18 Guangming Zhongjie, Chongwen District, Beijing, 100061, China
Doi:10.1002/poc.1506
(2009)Doi:10.1016/j.ejmech.2009.04.041
(2009)Doi:10.1021/jo00959a045
(1973)Doi:10.1021/ja00201a040
(1989)Doi:10.1246/bcsj.62.1528
(1989)Doi:10.1039/b613460b
(2006)