Journal of Organic Chemistry p. 2261 - 2262 (1989)
Update date:2022-08-04
Topics:
Yang, Ping-Fan
Ni, Zhi-Jie
Luh, Tien-Yau
A geminal dimethyl group is introduced regioselectively in excellent yield from the reactions of allylic dithioacetals and methylmagnesium iodide in the presence of 3 mol percent of NiCl2(dppe) in refluxing ether-benzene.
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