Chemical Communications p. 15760 - 15763 (2015)
Update date:2022-08-04
Topics:
Wong, Lawrence W-Y.
Kan, Jack W-H.
Nguyen, Thanh-Ha
Sung, Herman H-Y.
Li, Dang
Au-Yeung, Alex S-F.
Sharma, Rajpal
Lin, Zhenyang
Williams, Ian D.
Bis(mandelato)borate [B(Man)2]- (R- or S-) anions are simply prepared and appear widely effective for resolution of racemic cations. Three examples demonstrate their scope; the alkaloid tetrahydropalmatine (THP), 1,2-diaminopropane (1,2-dap) and the metal-organic complex [Co(phen)3]3+ are readily resolved, either by a facile one-pot procedure, or via counter-ion metathesis.
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