Journal of Fluorine Chemistry (2021)
Update date:2022-08-04
Topics:
Kirihara, Masayuki
Suzuki, Katsuya
Nakakura, Kana
Saito, Katsuya
Nakamura, Riho
Tujimoto, Kazuki
Sakamoto, Yugo
Kikkawa, You
Shimazu, Hideo
Kimura, Yoshikazu
Fluoroalkyl alcohols are effectivity oxidized to the corresponding fluoroalkyl carbonyl compounds by reaction with sodium hypochlorite pentahydrate in acetonitrile in the presence of acid and nitroxyl radical catalysts. Although the reaction proceeded slower under a nitroxyl radical catalyst- free condition, the desired carbonyl compounds were obtained in high yields. For the reaction with fluoroalkyl allylic alcohols, the corresponding α,β-epoxyketone hydrates were obtained in high yields.
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