Journal of Organic Chemistry p. 5202 - 5205 (1990)
Update date:2022-07-29
Topics:
Panetta, Charles A.
Garlick, Stephanie M.
Durst, H. Dupont
Longo, Frederick R.
Ward, J. Richard
The syntheses of five new 4-alkyl-2-iodosobenzoic acids (3) are described.The iodine atom was introduced by ortho-directed lithiation of 4-alkylbenzyl alcohols followed by treatment with I2.The catalytic effectiveness of each of the products in the hydrolysis of 4-nitrophenyl diphenyl phosphate in microemulsions was studied.The 4-methyl- and 4-ethyl-substituted products were each found to be significantly better catalysts than the standard nonalkylated 2-iodosobenzoic acid (3, R=H).These results would indicate that microemulsions of these materials may find use in detoxification procedures.
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