SYNTHESIS OF METHYL 2,6-DIDEOXY-4-THIO-α-D-RIBO-HEXOPYRANOSIDE, A NEW THIO SUGAR FOUND IN CALICHEMICINS

DOI: 10.1016/S0040-4039(01)80729-2

Source and publish data:

Tetrahedron Letters p. 4505 - 4506 (1989)

Update date:2022-08-04

Topics:

Authors:

Laak, Kai van

Scharf, Hans-Dieter

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Article abstract of DOI:10.1016/S0040-4039(01)80729-2

The radically induced rearrangement of the 3,4-O-thionocarbonate 4 leads to the two regioisomeric thiolcarbonates 5 and 6, respectively.Alkaline hydrolysis affords the title compound 7 and its regioisomer 8.

Full text of DOI:10.1016/S0040-4039(01)80729-2

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