Reaktionen mit sterisch gehinderten Stannylphosphinen: Synthese des ersten Zinn-substituierten Diphosphens

DOI: 10.1016/0022-328X(89)85097-1

Source and publish data:

Journal of Organometallic Chemistry p. C9 - C12 (1989)

Update date:2022-08-04

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Authors:

Haenssgen, Dieter

Aldenhoven, Heinz

Nieger, Martin

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Article abstract of DOI:10.1016/0022-328X(89)85097-1

A stable stannylated diphosphene, t-Bu3SnP=P(C6H2-2,4,6-t-Bu3), was prepared from 2,4,6-t-Bu3C6H2PCl2 and t-Bu3SnPHLi in the presence of Et3N.The novel diphosphene was characterized by NMR (1H, 31P, 119Sn) and mass spectroscopy and its molecular structure determined by X-ray crystallography (space group P2₁/c, Z=4).

Full text of DOI:10.1016/0022-328X(89)85097-1

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