Tetrahedron Letters p. 6005 - 6008 (1988)
Update date:2022-08-02
Topics:
Moody, Christopher, J.
Taylor, Roger, J.
Treatment of diazo sulphides with rhodium (II) acetate in benzene gives six- and seven-membered cyclic sulphonium ylides; although the S-benzyl and S-ethyl ylides can be isolated, they rearrange, or eliminate ethylene respectively, on heating; the S-allyl ylides cannot be isolated since they undergo spontaneous <2,3>-sigmatropic rearrangement.
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