Australian Journal of Chemistry p. 1729 - 1744 (1990)
Update date:2022-08-04
Topics:
Hartshorn, Michael P.
Hayman, Kamala A.
Martyn, Robert J.
Robinson, Ward T.
Vaughan, John
et al.
Reaction of mixture of 6-chlorocyclohexa-2,4-dienones (4) and (5) with chlorine in acetic acid gives the tetrachloro ketones (2) and (3), the major products of chlorination of 2,3,6-trimethylphenol (1a) or 4-chloro-2,3,6-trimethylphenol (1b).Reactions of this mixture of 6-chlorocyclohexa-2,4-dienones (4) and (5) in acetic acid with chlorine acetate, chlorine, chlorine in the presence of sodium acetate, and in benzene with nitrogen dioxide are described.X-ray crystal structure determinations are reported for compounds (3), (6)-(8) and (11)-(13).
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