Silylprotection in the solid-phase synthesis of N-linked neoglycopeptides. One-step deprotection of fully protected neoglycopeptides

DOI: 10.1016/S0040-4039(00)73692-6

Source and publish data:

Tetrahedron Letters p. 3315 - 3318 (1993)

Update date:2022-09-26

Topics:

Authors:

Christiansen-Brams

Meldal Meldal

Bock Bock

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Article abstract of DOI:10.1016/S0040-4039(00)73692-6

Silyl protection of the saccharide part in a building block for solid-phase synthesis of N-linked neoglycopeptides is described. Per-O-(trimethylsilylated) 1-amino-1-deoxy-D-glucitol 3 was reacted selectively with N(α)-Fmoc-Asp(Cl)-OPfp 1 and the resultin

Full text of DOI:10.1016/S0040-4039(00)73692-6

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