An improved, practical synthesis of the derivatives of 1-O-acetyl-2-deoxy-2-hydroxymethyl-D-erythrooxetanose, a key sugar moiety for the synthesis of oxetanosyl-N-glycoside

DOI: 10.1016/S0040-4020(01)90066-3

Source and publish data:

Tetrahedron p. 7703 - 7710 (1990)

Update date:2022-09-26

Topics:

Authors:

Nagai Nagai

Kato Kato

Takita Takita

Nishiyama

Yamamura

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Article abstract of DOI:10.1016/S0040-4020(01)90066-3

Intramolecular cyclization of the cis-epoxy-alcohol (6) with KOH in aq.DMSO provided predominantly the oxetane compound (7), which on oxidation followed by Baeyer-Villiger reaction gave 1-O-acetyl-D-erythrooxetanoses.

Full text of DOI:10.1016/S0040-4020(01)90066-3

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