Tetrahedron Letters p. 7093 - 7096 (1998)
Update date:2022-07-29
Topics:
Cahard, Dominique
Poirier, Jean-Marie
Duhamel, Pierre
The potassium dienolate of prenal obtained by treatment of the corresponding dienoxysilane with tBuOK was reacted with enaldehydes. In all cases a γ-specific reaction occurs. According to the reaction conditions a γ ;1,2 or a γ ;1,4 coupled product was selectively obtained with enals. The γ;1,2 reaction provided an efficient prenylation procedure. A short two- step synthesis of retinal is described.
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