Monatshefte fur Chemie p. 299 - 317 (1991)
Update date:2022-08-05
Topics:
Noe, Christian R.
Knollmueller, M.
Steinbauer, G.
Wagner, E.
Kuerner, H.
et al.
Enantiomerically pure 1,2-diols bearing optionally syn or anti configurated secondary hydroxylic groups are synthesized from acetal-protected cyanohydrins.After resolution of the diastereomers the cyanohydrins are converted into α-alkoxy-ketones by Grignard-reaction followed by reduction using common chelating or non-chelating agents.Among others syntheses of enantiomerically pure pheromones, endo-Brevicomin, exo-Brevicomin and Dispalure are given as examples.
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Doi:10.1016/0022-2860(91)80139-U
(1991)Doi:10.1021/ja2067324
(2012)Doi:10.1039/c1dt10931f
(2012)Doi:10.1002/anie.201914315
(2020)Doi:10.1039/c39910000708
(1991)Doi:10.1007/s11172-021-3165-8
(2021)
