Journal of Organic Chemistry p. 3348 - 3364 (2012)
Update date:2022-08-04
Topics:
Cheng, Ping
Clive, Derrick L. J.
Intramolecular conjugate displacement (ICD) has been applied to the Morita-Baylis-Hillman adducts formed from (5S)-5-(l-menthyloxy)-2(5H)-furanone and aldehydes that carry a protected β- or γ-amino group. DIBAL-H reduction of the resulting ICD products releases optically pure six- or seven-membered cyclic amines having a stereogenic center α to nitrogen.
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