Bulletin of the Academy of Sciences of the USSR Division of Chemical Science p. 2311 - 2313 (1991)
Update date:2022-08-05
Topics:
Dorokhov, V.A.
Komkov, A.V.
Vasil'ev, L.S.
Azarevich, O.G.
Gordeev, M.F.
1,1,1-Trifluoro-2-amino-3-acetyl-2-penten-4-one was obtained by the addition of acetylacetone to trifluoroacetonitrile in the presence of catalytic amounts of nickel acetylacetonate.The reaction of 1,1,1-trifluoro-2-amino-3-acetyl-2-penten-4-one with aryl isocyanates gave 1-aryl-5-acetyl-6-methyl-4-trifluoromethyl-1H-pyrimidin-2-ones.
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