Journal of Organic Chemistry p. 35 - 41 (2013)
Update date:2022-09-26
Topics: Catalyst Stereochemistry Synthetic route Total synthesis Enantioselective synthesis Protecting group Chirality Functional Group Interconversion
Liu, Xue-Kui
Ye, Jian-Liang
Ruan, Yuan-Ping
Li, Yu-Xiu
Huang, Pei-Qiang
An efficient synthesis of the Stemona alkaloid (-)-sessilifoliamide J (1) in 12 steps and 7.7% overall yield from the known building block 8 is presented. The synthesis features the Corey lactonization reaction and a highly diastereoselective α-methylation reaction to build the spirolactone moiety.
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