Journal of Organic Chemistry p. 11309 - 11317 (2018)
Update date:2022-07-30
Topics:
Vayer, Marie
Guillot, Régis
Bour, Christophe
Gandon, Vincent
A new method has been developed for the preparation of 3-bromo-1-phenylallenes from 7-alkynylcycloheptatrienes and N-bromosuccinimide. Trisubstituted bromoallenes were obtained at room temperature in moderate to excellent yields. Functionalization of the carbon-bromine bond via Pd- or Cu-catalyzed cross-coupling reactions easily provided substituted allenes.
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