2,3-DIMETHOXYPERHYDRO-1,4,2,3-DIOXADIAZINE: SYNTHESIS, CONFORMATION, AND CONVERSION TO 1-(2-HYDROXYETHOXY)-2-METHOXYDIAZENE-1-OXIDE. CRYSTAL STRUCTURE OF 1-(2-para-NITROBENZOYLOXY)ETHOXY>-2-METHOXYDIAZENE-1-OXIDE

DOI: 10.1007/BF00863376

Source and publish data:

Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.) p. 2074 - 2081 (1992)

Update date:2022-08-03

Topics:

Authors:

Rudchenko, V. F.

Ignatov, S. M.

Chervin, I. I.

Aliev, A. E.

Dekaprilevich, M. O.

et al. et al.

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Article abstract of DOI:10.1007/BF00863376

The oxidation of 1,2-bis(methoxyaminooxy)ethane (3) with PbO2 afforded 2,3-dimethoxyperhydro-1,4,2,3-dioxadiazine (4) in the form of the 55:45 mixture of the trans-4ee- and cis-4 isomers.The barrier of the ring conversion (ΔG₂₃₈^<*>=1

Full text of DOI:10.1007/BF00863376

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