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A stable compound with a formal tin-carbon double bond: The bis(2,4,6-triisopropylphenyl)(fluorenylidene)stannene

DOI: 10.1021/om00044a005

Source and publish data:

Organometallics p. 2748 - 2750 (1992)

Update date:2022-07-30

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Authors:

AnselmeAnselme

RanaivonjatovoRanaivonjatovo

EscudiéEscudié

CouretCouret

SatgéSatgé

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Article abstract of DOI:10.1021/om00044a005

Bis(2,4,6-triisopropylphenyl)(fluorenylidene)-stannene-diethyl ether (1a), a new stable compound with a formal tin-carbon double bond, has been synthesized by dehydrofluorination of the corresponding fluoro-stannane with tert-butyllithium; it has been characterized by NMR (δ(119Sn) + 288 ppm, δ(13C) +133.85 ppm) and UV spectroscopy (λmax 542 nm) and by electrophilic addition reactions to the tin-carbon unsaturation.

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Full text of DOI:10.1021/om00044a005

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