Synthesis of a Cell Wall Component of Haemophilus (Actinobacillus) Pleuropneumoniae Serotype 5

DOI: 10.1016/S0040-4020(01)81239-4

Source and publish data:

Tetrahedron p. 4649 - 4658 (1992)

Update date:2022-09-26

Topics: Synthesis Experimental terms Chemical terms Cell wall

Authors:

Klein, P. A. M. van der

Filemon, W.

Boons, G. J. P. H.

Veeneman, G. H.

Marel, G. A. van der

Boom, J. H. van

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Article abstract of DOI:10.1016/S0040-4020(01)81239-4

The disaccharide α-D-GlcNAcp-(1-5)-β-KDO-2-OCH2CH2CH2NH2 containing a spacer β-linked to KDO is prepared via iodonium ion-assisted glycosylation of a suitable KDO acceptor with ethyl 2-azido-2-deoxy-3,4-di-O-benzyl-1-thio-α/β-D-glucopyranoside.The key KDO building unit is synthesized in 7 steps starting with 2,3:5,6-di-O-isopropylidene-D-mannitol.

Full text of DOI:10.1016/S0040-4020(01)81239-4

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Product name:sodium (aminopropyl 5-O-(2-acetamido-2-deoxy-α-D-glucopyranosyl)-3-deoxy-β-D-manno-2-octulopyranosid)onate

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