Tetrahedron Letters p. 3927 - 3930 (1992)
Update date:2022-08-02
Topics:
Blackburn
Rosenberg
Yakovleva
Deuterium has been substituted into the methylene group of methylenebisphosphonic acid, MDP. Analysis of the phosphorus NMR spectrum of the product shows a linear high-frequency shift on sequential mono- and di-deuteriation. The corresponding tritium labelling of MDP achieved a specific activity of 30 mCi/mmol.
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