Tetrahedron p. 8253 - 8262 (1992)
Update date:2022-09-26
Topics:
Shono, Tatsuya
Terauchi, Jun
Kitayama, Kenji
Takeshima, Yo-Ichiro
Masumura, Yoshihiro
Electroreduction of nitriles gave the corresponding decyanated products when Zn was used as the material of cathode in aprotic solvent (DMF or MeCN) containing Et4NOTs as a supporting electrolyte. Alkylation of amines at the α-position was effectively achieved by cyanation of amines at the α-position, and α-alkylation of the resultant α-amino nitriles followed by the electroreductive decyanation.
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