A novel convergent strategy for the construction of oligosaccharides using TIPS-protected glycosides. Synthesis of fragments related to glycolipids of Mycobacterium smegmatis

DOI: 10.1016/S0040-4039(00)60999-1

Source and publish data:

Tetrahedron Letters p. 6615 - 6618 (1992)

Update date:2022-08-04

Topics:

Authors:

Ziegler, Thomas

Eckhardt, Elisabeth

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1016/S0040-4039(00)60999-1

4,6-O-Pyruvylated glucosides 1 were converted to the corresponding glucosyl fluorides 3 and 2,3-O-TIPS-protected glucopyranosides 5, respectively. Lewis-acid-catalyzed coupling of 3 and 5 afforded the pyruvylated disaccharides 6 one of which was further converted via the dissacharide donor 8 to di- and trisaccharide fragments of Mycobacterium smegmatis.

Full text of DOI:10.1016/S0040-4039(00)60999-1

Products guided by the article

Product name:2-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-3-O-methyl-D-glucopyranose

Cas No:146530-73-6

R&D Labs maybe for 146530-73-6

Shanghai PotentPharm Science and Technology Co.,Ltd

Contact:86-021-51969655

Address:Unit B, Building 18, No.300, Chuantu Rd,Pudong District, Shanghai 201202, China
SuZhou Hua-Emy Chemical Import and Export Co., LTD.

Contact:+86-512-88804994; +86-512-88804550;

Address:710, Building B, International Trade Center, 12 Huanghelu, Changshu, Jiangsu,China
KODI CHEMICAL CO., LTD

Contact:021

Address:Pudong
Watson International Ltd

Contact:+44 (0)2036089360-31

Address:Chanceryhouse,Chancery Lan
APOLLO HEALTHCARE RESOURCES

Contact:+65 9658 0999

Address:26 Sin Ming Lane, Midview City, #05-118, Singapore 573971

Relevant to this article

Diels-Alder Reactions of α-Substituted Styrenes with p-Benzoquinone

Doi:10.1021/jo00086a046
(1994)
Isolation and characterization of novel degradation products in cilnidipine by LC-QTOF-MS/MS, LCMSⁿ, 2D-NMR and FTIR

Doi:10.1039/c7nj02781h
(2018)
Doi:10.1021/jo01265a601
(1968)
Synthesis, Characterization and Crystal Structures of 1,7-dioxa-4-thia-10-azacyclododecane (<12>aneNO2S) and aneNO2S)(NO3)2>

Doi:10.1039/DT9930000625
(1993)
Synthesis of carbazoles via one-pot copper-catalyzed amine insertion into cyclic diphenyleneiodoniums as a strategy to generate a drug-like chemical library

Doi:10.1002/adsc.201300271
(2013)
γ-Selectivity in the Ceric Ammonium Nitrate Promoted Oxidative Addition of Silyl Dienol Ethers to Silyl Enol Ethers

Doi:10.1016/S0040-4039(00)61663-5
(1993)

Article Doi