Macrocyclic ethers by free radical cyclizations

Article abstract of DOI:10.1080/00397919708004135

Tin hydride reduction of ω-iodo-polyoxaalkyl acrylates 1 using syringe pump addition of both reactants to a solution of AIBN in benzene at 80°C afforded the corresponding cyclic polyethers in excellent yields.

Full text of DOI:10.1080/00397919708004135

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Synthetic Communications: An
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Organic Chemistry
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Macrocyclic Ethers by Free
Radical Cyclizations
Annie Philippon a , Jingchao Tao a , David Tétard a ,
Marie Degueil-Castaing a & Bernard Maillard a
a Laboratoire de Chimie Organique et
Organométallique, associé au CNRS URA 35,
Université Bordeaux 1 , F-33405, TALENCE-Cedex,
France
Published online: 22 Aug 2006.
To cite this article: Annie Philippon , Jingchao Tao , David Tétard , Marie Degueil-
Castaing & Bernard Maillard (1997) Macrocyclic Ethers by Free Radical Cyclizations,
Synthetic Communications: An International Journal for Rapid Communication of
Synthetic Organic Chemistry, 27:15, 2651-2682, DOI: 10.1080/00397919708004135
To link to this article: http://dx.doi.org/10.1080/00397919708004135
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