Bulletin of the Chemical Society of Japan p. 246 - 250 (1994)
Update date:2022-08-05
Topics:
Yamashita, Toshiaki
Tanabe, Kimiko
Yamano, Katsuhiko
Yasuda, Masahide
Shima, Kensuke
Photoamination of 2-alkoxynaphthalenes (1) with ammonia and primary alkylamines were performed by irradiating an acetonitrile-water solution containing 1, an amine, and m-dicyanobenzene to give 1-alkylamino-2-alkoxy-1,4-dihydronaphthalene (2) in relatively good yields.The conversion of 2 to N-acetyl-1-alkylamino-2-tetralones was performed by acetylation with Ac2O by a treatment with BF3*OEt2.
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