Carbohydrate Research p. 9 - 20 (1984)
Update date:2022-08-05
Topics:
Inoue, Yoshio
Okuda, Takehiro
Kuan, Fu-Hua
Chujo, Riichiro
The chemical shifts and line-shapes of cross-polarisation-magic-angle sample spinning 13C-n.m.r. resonances have been analysed for p-nitrophenol, p-hydroxybenzoic acid, benzoic acid, and m-nitrophenol in the solid state and likewise for inclusion complexes with host cyclomalto-hexaose and -heptaose.The trends of the chemical-shift displacements induced by complexation with the cycloamyloses in the solid state did not fully correspond with those for solutions.The line-shapes showed evidence of the rotational motion of the benzene compounds in the cavity of cyclomaltohexaose, but not in that of cyclomaltoheptaose.
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